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Palladium
Acetate
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Palladium(II) acetate is a
chemical compound of palladium described by the formula Pd(O2CCH3)2 or
Pd(OAc)2. It is considered more reactive than the analogous platinum
compound. It is soluble in many organic solvents.
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Palladium (II) acetate was found
to be an effective catalyst, yielding 100% product for several aldehydes
used. Lower yields were attributed to altering the reflux time,
distillation processes, and attempting to reuse the catalyst.
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Palladium acetate can be
prepared by refluxing palladium sponge with hot glacial acetic acid and
nitric acid. An excess of palladium sponge is used to prevent
contamination by PdNO3·OAc.
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Palladium acetate is a catalyst
for many organic reactions by combining with many common classes of
organic compounds such as alkenes, dienes, and alkyl, aryl, and vinyl
halides to form reactive adducts.
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Palladium Acetate is a
moderately water soluble crystalline Palladium source that decomposes to
Palladium oxide on heating. It is generally immediately available in
most volumes.
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Nanoparticles of palladium and
palladium containing intermetallic compounds (IMCs) have unique
applications: sensors , catalysts , active membranes and etc.
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Thermal decomposition of solids
is an important field of solid state chemistry with wide technical
applications. Metal acetates represent an important class of the
compounds with wide technical and biological applications. Palladium
acetate has a wide application as a catalyst in organic synthesis and
petrochemical industries.
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Palladium has a rich
organometallic chemistry which has developed over the past twenty-five
years. While palladium is not unique in its ability to carry out a wide
range of carbon-carbon bond forming reactions, its ver- satility has
resulted in an increasing effort being made towards the use of palladium
reagents in organic synthesis in academic and industrial research
laboratories.
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Widely used procedures such as
the Heck, Suzuki and Sonogashira cross-coupling reactions and
Buckwald-Hartwig aminations most commonly employ a palladium-based
catalyst.
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